LI Pengrui *,REN Chunjiang,ZHANG Junyun,et al.Effect of Electroplating Parameters on the Performance of Electroplating Nickel Layer[J].Plating & Finishing,2022,(2):26-29.[doi:10.3969/j.issn.1001-3849.2022.02.006]
电镀参数对电镀镍层性能的影响
- Title:
- Effect of Electroplating Parameters on the Performance of Electroplating Nickel Layer
- 分类号:
- TQ153.2
- 文献标志码:
- A
- 摘要:
- 采用脉冲电流方法制备电镀镍层，并利用扫描电镜、光学轮廓仪、硬度计等测试方法研究了电镀参数中的溶 液温度和 pH 对电镀镍层的表面形貌、粗糙度、显微硬度和 SiC/Ni 刻蚀选择比的影响。结果表明：当镀液温度在 45 ～ 60 ℃ 时，镀镍层表面形貌变化不大，但是随着镀液温度的升高和镀液 pH 的增大，粗糙度呈先减小后增大的趋势，显微硬度和 SiC/Ni 刻蚀选择比均呈先增大后减小的趋势。电镀液温度为 55 ℃ ， pH 在 4.0 ～ 4.4 时，可获得具有良好的质量、显微硬度且 SiC/Ni 刻蚀选择比的镍镀层。
- Abstract:
- The electroplating nickel layer was prepared by pulse current method ， and the effects of solution temperature and pH on the surface morphology ， roughness ， microhardness and SiC/Ni etching selectivity ratio of electroplating nickel layer were investigated by scanning electron microscope ， optical profilometer and hardness tester. The results showed that when the bath temperature increased from 45 ℃ to 60 ℃ ， the surface morphology of nickel plating layer had little change ， but with the increase of bath temperature and pH ， the roughness decreased first and then increased ， the microhardness and the SiC/Ni etching selection ratio both increased first and then decreased. When the bath temperature was 55 ℃ and pH was 4.0‐4.4 ， the nickel coatings with good quality ， microhardness and etching selectivity ratio of SiC/Ni can be obtained.
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备注/Memo
收稿日期： 2021-09-07 修回日期： 2021-10-15 作者简介： 李彭瑞（ 1988 —），男，硕士，工程师， email ： pary_li@163.com