[1]侯攀超,杨 玥,周景淼,等.ZnO/GO复合薄膜电极的制备及其耐腐蚀性能[J].电镀与精饰,2024,(10):50-55.
　Hou Panchao,Yang Yue,Zhou Jingmiao,et al.Preparation and corrosion resistance of ZnO/GO composite thin film electrodes[J].Plating & Finishing,2024,(10):50-55.
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ZnO/GO复合薄膜电极的制备及其耐腐蚀性能()

《电镀与精饰》[ISSN:1001-3849/CN:12-1096/TG]

卷:
期数:
2024年10
页码:
50-55
栏目:
出版日期:
2024-10-15

文章信息/Info

Title:
Preparation and corrosion resistance of ZnO/GO composite thin film electrodes
作者:
侯攀超1; 杨 玥1; 周景淼1; 郭虹妍2; 王天昊3; 童贞祥4; 冷华章4; 李家军4; 王继文5; 宋振兴1
(1. 天津科技大学 理学院,天津 300457 ;2. 天津科技大学 海洋与环境学院,天津 300457 ;3. 天津市飞鸽集团联合化工厂,天津 300163 ;4. 扬中永新镀业有限公司,江苏 镇江 212200 ;5. 沈阳亿航精饰环保有限公司,辽宁 沈阳 110000 )
Author(s):
Hou Panchao 1;  Yang Yue1;  Zhou Jingmiao 1 ;  Guo Hongyan 2;  Wang Tianhao3;  Tong Zhenxiang4;  Leng Huazhang 4;  Li Jiajun4;  Wang Jiwen5;  Song Zhenxing1*
(1. College of Science, Tianjin University of Science and Technology, Tianjin 300457, China; 2. College of Marine and Environmental Sciences, Tianjin University of Science and Technology, Tianjin 300457, China; 3. Tianjin Feige Group Joint Chemical Factory, Tianjin 300163, China; 4. Yangzhong Yongxin Plating Industrial Co., Ltd., Zhenjiang 212200, China; 5. Shenyang Yihang Finishing Environmental Protection Co., Ltd., Shenyang 110000, China )
关键词:
氧化锌; 氧化石墨烯; 复合薄膜; 电催化; 溶胶-凝胶法
Keywords:
zinc oxide;  graphene oxide;  composite films;  electrocatalysis;  sol-gel method
分类号:
TQ153.2
文献标志码:
A
摘要:
本文利用溶胶-凝胶法制备了氧化锌/氧化石墨烯（GO）复合薄膜材料。通过扫描电子显微镜发现复合薄膜中的GO颗粒之间无明显间隙，致密性良好。由傅里叶红外光谱测试证实GO在氧化锌薄膜中成功掺杂。通过阳极极化测试发现，相比于氧化锌薄膜，ZnO/GO复合薄膜的腐蚀电位值正移，腐蚀电流密度值减小。交流阻抗测试说明，GO的掺杂提高了复合薄膜的耐腐蚀性能，经450 ℃退火的薄膜样品耐腐蚀性能最佳。线性扫描伏安曲线表明，ZnO/GO复合薄膜的电流密度高于ZnO薄膜，说明ZnO的复合提高了薄膜材料的电催化活性。
Abstract:
In this paper, ZnO/ graphene oxide (GO) composite thin film materials were prepared by sol-gel method. It was found by scanning electron microscopy that there was no obvious gap between the GO particles in the composite film, and the density was good. The successful doping of GO in the ZnO film was confirmed by Fourier infrared spectroscopy test. By anodic polarization test, it was found that the corrosion potential value of ZnO/GO composite film was positively shifted and the value of corrosion current density was decreased compared with ZnO film. The AC impedance test indicated that the corrosion resistance of the composite films was improved by doping of GO. The best corrosion resistance was obtained for the film samples annealed at 450 ℃. Linear scanning voltammetry curves showed that the current density of ZnO/GO composite films was higher than that of ZnO films, indicating that the electrocatalytic activity of the film material was improved by composite of ZnO particles.

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更新日期/Last Update: 2024-10-16