HU Shuilian*,PI Zhichao.An Analysis and Treatment of Malfunctions Occurred in Nickel Plating Solution[J].Plating & Finishing,2020,(9):46-48.
一例电镀镍故障的原因分析和排除
- Title:
- An Analysis and Treatment of Malfunctions Occurred in Nickel Plating Solution
- Keywords:
- nickel plating black rough fault
- 文献标志码:
- A
- 摘要:
- 针对一例镍镀层表面发黑、粗糙，分散能力差故障进行了分析，并提出了故障处理方法。通过赫尔槽试验，确定了除杂剂的添加量；通过双氧水氧化及活性炭过滤，去除了槽液中的有机物；通过电解去除了槽液中络合金属离子；最后通过调整槽液成分含量于规定范围，解决了试镀故障。
- Abstract:
- In this paper, a trouble of poor scattered ability and the nickel plating with black and rough surface was analyzed, and fault processing methods are put forward. Through hall cell test, the content of removing impurity agent was confirmed. By adding hydrogen peroxide oxidation and activated carbon filter, the organic matter in the bath were removed. The complexation metal ions in bath were removed by electrolysis. Finally, the component content of bath was adjusted to the prescribed scope and the trouble of plating nickel was resolved.
参考文献/References:
[1] 程秀云. 电镀技术[M]. 北京: 化学工业出版社, 2003.
[2] 刘德鑫, 彭晓杰, 赵桂兰, 等.氨基磺酸盐电镀镍层内应力的影响因素研究[J]. 电镀与精饰, 2017, 39(8): 10-14.
Liu D X, Peng X J, Zhao G L, et al. Study on influence factors of internal stress of nickel coatings electroplated using aminosulfonate[J]. Plating and Finishing, 2017, 39(8): 10-14 (in Chinese).
[3] 郭崇武, 向思杰. 一次电镀装饰铬故障的排除[J]. 电镀与精饰, 2010, 32(2): 24-26.
Guo C W, Xiang S J. Elimination of a decorative chromium plating malfunction [J]. Plating and Finishing, 2010, 32(2): 24-26 (in Chinese).
[4] 郭崇武, 王小东. 氯化钾无氰镀镉故障分析与处理[J]. 电镀与涂饰, 2017, 36(23): 1271-1272.
Guo C W, Wang X D. Analysis and treatment of malfunctions occurred in cyanide-free potassium chloride cadmium electroplating[J]. Electroplating & Finishing, 2017, 36(23): 1271-1272 (in Chinese).
[5] 郭崇武. 镀镍槽糖精钠过量引起的质量事故分析[J]. 电镀与涂饰, 2014, 33(3): 118-119.
Guo C W. Analysis on a plating quality accident caused by excessive sodium saccharin in nickel plating bath[J]. Electroplating & Finishing, 2014, 33(3): 118-119 (in Chinese).
[6] 张允诚, 胡如南, 向荣, 等. 电镀手册（上册）[M]. 北京: 国防工业出版社, 1997: 317-319.
[7] 张业明, 陈志量, 郝龙, 等. 硫酸盐镀铜的故障分析及修复[J]. 材料保护, 2007, 40(7): 67-69.
Zhang Y M, Chen Z L, Hao L, et al. Trouble-shooting technology for copper electroplating from sulfate bath[J]. Materials Protection, 2007, 40(7): 67-69 (in Chinese).
[8] 袁诗璞, 李铭华, 黄渭澄, 等. 电镀技术[M]. 成都: 四川人民出版社, 1982.
[9] 奚兵. 电镀脱皮故障的原因分析[J]. 电镀与涂饰, 2009, 28(12): 23-24.
Xi B. Cause analysis on peeling in electroplating[J]. Electroplating & Finishing, 2009, 28(12): 23-24 (in Chinese).
相似文献/References:
[1]仝晓刚*. 某半刚性电缆组件腐蚀分析与防护 [J].电镀与精饰,2022,(9):15.[doi:10.3969/j.issn.1001-3849.2022.09.003]
TONG Xiaogang *.Corrosion Analysis and Protection of a Semi-Rigid Cable Assembly[J].Plating & Finishing,2022,(9):15.[doi:10.3969/j.issn.1001-3849.2022.09.003]
[2]詹兴刚,胡军林,刘 燕*,等.航空发动机用离子镀银紧固件的耐酸性盐雾性能研究[J].电镀与精饰,2022,(11):12.[doi:10.3969/j.issn.1001-3849.2022.11.003]
ZHAN Xinggang,HU Junlin,LIU Yan*,et al.Study on Acid Salt Spray Corrosion Resistance of Fasteners with Vacuum ion Plated Silver Coating used on Aero Engine[J].Plating & Finishing,2022,(9):12.[doi:10.3969/j.issn.1001-3849.2022.11.003]