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[1]姚伦芳,罗雪芳,刘定富*.热处理温度对电沉积Ni-W-B合金镀层性能的影响[J].电镀与精饰,2022,(9):93-96.[doi:10.3969/j.issn.1001-3849.2022.09.016]
　YAO Lunfang,LUO Xuefang,LIU Dingfu*.Effect of Heat Treatment on the Coating Properties of Electrodeposited Ni-W-B Alloy[J].Plating & Finishing,2022,(9):93-96.[doi:10.3969/j.issn.1001-3849.2022.09.016]
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热处理温度对电沉积Ni-W-B合金镀层性能的影响

《电镀与精饰》[ISSN:1001-3849/CN:12-1096/TG] 卷: 期数: 2022年9 页码: 93-96 栏目: 出版日期: 2022-09-15
Title:
Effect of Heat Treatment on the Coating Properties of Electrodeposited Ni-W-B Alloy
作者:
（1.贵州省环境工程评估中心， 贵州 贵阳 550002； 2.贵州大学 化学与化工学院， 贵州 贵阳 550025）
Author(s):
( 1.Guizhou Environmental Engineering Assessment Center Guiyang 550002 China 2.College of Chemistry and Chemical Engineering Guizhou University Guiyang 550025 China )
关键词:
电沉积;  Ni-W-B 合金; 硬度; 耐蚀性
Keywords:
electrodeposition ;  Ni-W-B alloy ;  hardness ;  corrosion resistance
分类号:
TQ153.2
DOI:
10.3969/j.issn.1001-3849.2022.09.016
文献标志码:
A
摘要:
热处理温度对镀层性能有直接影响。本文以黄铜为基材，在镀液中电沉积 Ni-W-B 合金镀层，然后研究热处理温度变化对镀层性能的影响。采用扫描电镜（ SEM ）、 X 射线衍射（ XRD ）、百格刀、硬度计对镀层表面形貌、组织结构、附着力及硬度进行测试分析。结果表明，热处理使 Ni-W-B 合金镀层从非晶态结构逐渐转变为晶态结构，当热处理温度为 500 ℃ 时，镀层的表面最为致密，镀层与基体间结合良好（ ISO 等级为 1 ， ASTM 等级为 4B ）；镀层的硬度从 499.1 HV 增加到最大值 960.5 HV ，增幅达 92.4% ，与镀铬层相当。
Abstract:
： Heat treatment temperature has a direct effect on coating properties. This paper uses brass as the substrate and electrodeposits Ni-W-B alloy plating in the plating solution ， and then investigates the effect of heat treatment temperature on the plating properties. Scanning electron microscope ， diffraction of X-rays ， baguette and hardness tester are used to test and analyze the surface morphology ， structure ， adhesion and hardness of the plating. The results show that the heat treatment gradually transforms the Ni-W-B alloy coating from an amorphous structure to a crystalline structure. When the heat treatment temperature is 500 °C ， the surface of the coating is the densest ， the bond between the coating and the substrate is good （ ISO grade 1 ， ASTM grade 4B ）， and the hardness of the coating increases by 92.4% ， reaching a maximum value of 960.5 HV ， which is comparable to that of the chromium coating.

参考文献/References:



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备注/Memo

收稿日期： 2022-07-18 修回日期： 2022-08-05 著者简介 ： 姚伦芳（ 1987 ―），男，硕士，主要从事生态环境保护技术咨询工作， email ： 670937300@qq.com 通讯著者 ： 刘定富， email ： liuxiao8989@163.com?/html>

更新日期/Last Update: 2022-09-08