[1]毛望军*,高志廷.齿轮钢电沉积Ni-W/MoS2自润滑复合镀层及性能研究[J].电镀与精饰,2023,(4):31-37.[doi:10.3969/j.issn.1001-3849.2023.04.006]
　Mao Wangjun*,Gao Zhiting.Study on properties of Ni-W/MoS 2 self-lubricating composite coatings electrodeposited on gear steel[J].Plating & Finishing,2023,(4):31-37.[doi:10.3969/j.issn.1001-3849.2023.04.006]
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齿轮钢电沉积Ni-W/MoS2自润滑复合镀层及性能研究
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《电镀与精饰》[ISSN:1001-3849/CN:12-1096/TG]

卷:
期数:
2023年4
页码:
31-37
栏目:
出版日期:
2023-04-15

文章信息/Info

Title:
Study on properties of Ni-W/MoS 2 self-lubricating composite coatings electrodeposited on gear steel
作者:
（1.河南机电职业学院 智能工程学院，河南 郑州 451191； 2.北京理工大学 材料学院，北京 100081）
Author(s):
（1.School of Intelligent Engineering， Henan Mechanical and Electrical Vocational College，Zhengzhou 451191， China； 2.School of Materials Science and Engineering， Beijing Institute of Technology， Beijing 100081， China）

关键词:
Ni-W/MoS 2 自润滑复合镀层; 电沉积; 齿轮钢;  MoS 2 颗粒质量浓度; 耐磨性能
Keywords:
Ni-W/MoS 2 self-lubricating composite coating ;  electrodeposition ;  gear steel ;  mass concentration of MoS 2 particles ;  wear resistance
分类号:
TQ153
DOI:
10.3969/j.issn.1001-3849.2023.04.006
文献标志码:
A
摘要:
采用电沉积工艺在制造齿轮常用的 40Cr 钢表面制备掺杂 MoS 2 颗粒的 Ni-W/MoS 2 自润滑复合镀层，并研究 MoS 2 颗粒对复合镀层表面形貌、晶相结构、显微硬度和耐磨性能的影响。结果表明： Ni-W/MoS 2 自润滑复合镀层完整覆盖 40Cr 钢表面，主要成分为 Ni 、 W 、 Mo 和 S 元素，存在 4 个 Ni 的衍射峰并且都呈现（ 220 ）晶面择优取向。镀液中 MoS 2 颗粒质量浓度变化导致镀层的晶粒形态及致密性显现出差异， MoS 2 颗粒含量呈现先升高后降低趋势，造成显微硬度先增大后减小，耐磨性能先改善后变差。当镀液中 MoS 2 颗粒质量浓度为 5 g/L ， Ni-W/MoS 2 复合镀层中 MoS 2 颗粒含量达到 4.17% ，形成条状与乳突状不同形态的晶粒，结合更紧密，其硬度达到 607.5 HV ，表面磨痕宽度仅为 420 μ m ，表现出良好的耐磨性能，能起到较理想的减摩作用，从而显著提高 40Cr 钢的耐磨性能。
Abstract:
： The Ni-W/MoS 2 self-lubricating composite coatings doped with MoS 2 particles were prepared on 40Cr steel commonly used for gear manufacturing by electrodeposition ， and the effect of MoS 2 particles on the surface morphology ， crystal structure ， microhardness and wear resistance of the composite coatings was investigated. The results show that the Ni-W/MoS 2 self-lubricating composite coating covers the surface of 40Cr steel completely ， the main components are Ni ， W ， Mo and S elements ， and there are four Ni diffraction peaks ， showing the preferred orientation of （ 220 ） crystal plane. Variation of the mass concentration of MoS 2 particles in the plating solution causes the difference in the grain morphology and compactness of the composite coating ， and the content of MoS 2 particles firstly increases and then decreases ， resulting in the microhardness first increases and then decreases ， and the wear resistance gradually improves and then deteriorates. When the mass concentration of MoS 2 particles in the plating solution is 5 g/L ， the Ni-W/MoS 2 composite coating with the highest MoS 2 particles content up to 4.17% ， and the strip and mastoid grains of different morphology are closely bonded ， the hardness reaches 607.5 HV ， and the width of surface wear mark is only 420 μ m. The Ni-W/MoS 2 composite coating exhibiting good wear resistance ， and it can play an ideal anti-friction effect and significantly improve the wear resistance of 40Cr steel.

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备注/Memo

备注/Memo:
收稿日期： 2023-03-04 修回日期： 2023-03-29 * 通信作者： 毛望军（ 1971 —），高级实验师，主要研究方向：机械制造、金属表面改性、微纳加工技术等， email ： mwj020926@126.com 基金项目： 河南省科学技术厅项目（ 162102210320 ）?/html>
更新日期/Last Update: 2023-04-14