[1]李 鹏,苗 旺,米佳鑫,等.doi: 10.3969/j.issn.1001-3849.2025.10.0110Cr13Ni5Mo不锈钢表面化学镀Ni-P-Si工艺[J].电镀与精饰,2025,(10):74-82.
　Jing Zonghao,Yang Yuyun,Wang Yongdong.Process of electroless Ni-P-Si plating on the surface of 0Cr13Ni5Mo stainless steel Li Peng1, Miao Wang1, Mi Jiaxin1, Zheng Jiaqi1, Ren Yuanda2*,[J].Plating & Finishing,2025,(10):74-82.
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doi: 10.3969/j.issn.1001-3849.2025.10.0110Cr13Ni5Mo不锈钢表面化学镀Ni-P-Si工艺()

《电镀与精饰》[ISSN:1001-3849/CN:12-1096/TG]

卷:
期数:
2025年10
页码:
74-82
栏目:
出版日期:
2025-10-31

文章信息/Info

Title:
Process of electroless Ni-P-Si plating on the surface of 0Cr13Ni5Mo stainless steel Li Peng1, Miao Wang1, Mi Jiaxin1, Zheng Jiaqi1, Ren Yuanda2*,
作者:
李 鹏1; 苗 旺1; 米佳鑫1; 郑嘉琪1; 任远达2; 景宗浩2; 杨雨云3; 王永东2
(1. 哈尔滨电机厂有限责任公司,黑龙江 哈尔滨 150002 ;2. 黑龙江科技大学 材料科学与工程学院,黑龙江 哈尔滨 150022 ;3. 哈尔滨工程大学 材料科学与化学工程学院,黑龙江 哈尔滨 150001)
Author(s):
Jing Zonghao2;  Yang Yuyun3;  Wang Yongdong2
(1. Harbin Electric Machinery Factory Co., Ltd., Harbin 150002, China; 2. College of Materials Science and Engineering, Heilongjiang University of Science and Technology, Harbin 150022, China; 3. College of Materials Science and Chemical Engineering, Harbin Engineering University, Harbin 150001, China)
关键词:
化学镀; Ni-P-Si; 显微硬度; 耐磨性
Keywords:
chemical plating;  Ni-P-Si;  microhardness;  wear resistance
分类号:
TG174.4
文献标志码:
A
摘要:
化学镀方法作为材料表面改性技术，可以提升材料表面的耐磨等性能。本文研究了镀液温度、pH和施镀时间对化学镀层组织和性能的影响。采用扫描电镜(SEM)、能谱仪(EDS)和X射线衍射仪(XRD)观察镀层表面的微观形貌，分析镀层的成分变化并分析镀层的物相。对镀层进行了热处理，测试其显微硬度和耐磨性。结果表明：镀液温度为85 ℃、pH为5.5时，镀层表面光滑平整。施镀时间为60 min时，镀层厚度达到40 μm，且呈现出良好的致密性，无明显的开裂缺陷。在最佳电镀参数，即镀液温度85 ℃、pH为5.5、施镀时间60 min以及热处理温度320 ℃、保温10 min条件下，镀层的显微硬度达1 458.88 HV。
Abstract:
The chemical plating method, as a material surface modification technology, can improve the wear resistance and other properties of the material surface. The effects of plating solution temperature, pH value, and plating time on the microstructure and properties of chemical coatings were investigated in this article. Scanning electron microscopy (SEM) was used to observe the microstructure of the coating surface, energy dispersive spectroscopy (EDS) was used to analyze the compositional changes of the coating, and X-ray diffraction (XRD) was used to analyze the phase of the coating. The coating was subjected to heat treatment and its microhardness and wear resistance were tested. The research results indicate that when the plating solution temperature is 85 ℃ and the pH value is 5.5, the surface of the coating is smooth and flat. When the plating time is 60 min, the coating thickness reaches 40 μm and exhibits good density without obvious cracking defects. Under the optimal process parameters of 85 ℃, pH of 5.5, coating time of 60 min, heat treatment at 320 ℃ and insulation for 10 min, the microhardness of the coating reached 1 458.88 HV

参考文献/References:

[1].孙伟清, 陈微, 王玮琪. 镁合金建筑模板的表面化学镀与耐蚀性能[J]. 电镀与精饰, 2024, 46(10): 34-41.
[2].阚金锋, 吕成伟, 马放, 等. 化学镀Ni-P镀层耐蚀性的研究进展[J]. 有色金属加工, 2024, 53(4): 55-62.
[3].晁爽, 曹晶晶, 李河宗, 等. 微纳SiCP对化学镀Ni-P-SiCP复合镀层组织和性能的影响[J]. 稀有金属材料与工程, 2024, 53(10): 2723-2734.
[4].周柏玉, 黄仁超. 低浓度硫酸铜对化学镀Ni-P镀层微观结构及性能的影响[J]. 材料保护, 2024, 57(6): 147-153.
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更新日期/Last Update: 2025-10-17